ORGANIC CHEMISTRY 2325 LABORATORY EXPERIMENT SCHEDULE
Spring 2009

Text: Introduction to Organic Laboaratory Techniques and Small Scale Approach - Pavia, Lampman, Kris and Engel; 2nd Edition

Experiment #  Experiment #  in text / Title   Reference  to text
- Introductory and safety issues, proper care and use of glassware, and laboratory techniques.
- Notebook.
- Post-lab: outline a proper step-wise procedure for washing and drying glassware.
2-39
Tech 1, 2.1, 2.2
Syllabus and Safety Agreement
Exp # 4, #10
Handouts

#34 - Preparation of Benzil
294-296
3
#43 - Nitration of Methyl Benzoate
352-355
4
#36 (1st Ed.) - Methyl Orange
1st Ed.: 318-323
5
#36 - Preparation of Grignard Reagent
303-309
6
#36A - Triphenylmethanol
309-311
7
#13 - Methyl Salicylate
96-101
8
#38 - Aldol Condensation
322-326
9
#39 - Michael and Aldol Condensation
326-330
10
#44 (1st Ed.) - PABA
1st Ed.: 383-388
11
#44 - Benzocain
361-363
12
#45 - "OFF" Insect Repellant
370-375
13
#55 - Make-Up Lab - Identification of Unknowns
B - no nitro or cyano groups, no sodium fusion
C - no bromine test
D - no chromic acid test
F - no bromine/water test
G - do only IR
H - do only IR
Check out: EVERYBODY MUST ATTEND CHECK OUT!