ORGANIC CHEMISTRY 2325
SUMMER LABORATORY EXPERIMENT SCHEDULE
Summer 2007

Text: Introduction to Organic Laboratory Techniques and Small Scale Approach - Pavia, Lampman, Kris, and Engel; Second Edition.

Experiment #  Experiment #  in text / Title   Reference  to text
1 
  1. Introductory and safety issues.
  2. Care and use of glassware.
  3. Laboratory Techniques.
  4. Calibration of the thermometer.
  5. Notebook.
  6. Exp. # 43: Nitration of Methyl Benzoate
  1. pages 2-39
  2. techniques 1, 2.1, 2.2
  4. Safety Agreement
  5. pages 352-355
2 

Exp.# 36: Preparation of Grignard Reagent (continue until ok to stop in #36a)

pages 303-309
3 

Exp. #36A: Triphenylmethanol

pages 309-311
4
 Exp.# 36 (1st Ed.): Methyl Orange pages 318-323 (1st Ed.)
5
 Exp. # 44 Benzocain pages 361-363
6
 Exp.# 34: Preparation of a Benzil pages 294-296
7
 Exp.# 39 Michael and Aldol Condensation Reactions pages 326-329
8
 Exp. # 44 DEET "OFF®" Insect Repellant pages 370-375
9
 Exp. # 44 (1st Ed.): PABA pages 383-388
10
  1. Equipment checkout
  2. Everyone attends checkout
  3. Make-up lab:  Exp. # 55: Identification of Unknowns

B - no nitro or cyano groups, no Na fusion
C- no Br2 test
D - no chromic acid test
F - no Br2/H2O test
G - do IR only
H - do IR only

 pages  468-511