ORGANIC CHEMISTRY 2315
LABORATORY EXPERIMENT SCHEDULE
SUMMER 2007

Text: Introduction to Organic Laboratory Techniques and Small Scale Approach - Pavia, Lampman, Kris, and Engel; Second Edition.

Experiment #  Experiment #  in text / Title   Reference  to text
1 
  1. Introductory and safety issues.
  2. Proper care and use of glassware and laboratory techniques.
  3. Notebook.
  4. Calibration of the thermometer.
  5. Post-lab: percent yield determination
  1. pages 2-39
  2. techniques 1, 2.1, 2.2
  4. Safety Agreement
2 

Exp.# 1 (1st Ed.): Isolation of an Active Ingredient in an Analgesic Drug.

Start #17 - Ethanol from Sucrose (use balloon as CO2 trap)

 1st Ed. 42-46
 

pages 135-139
3
 Finish Exp.#17 Ethanol from Sucrose pages 135-139
4
 Exp. #12: Isopentyl Acetate pages 93-96
5
 Exp. # 26: Methyl Stearate from Methyl Oleate 
 the hydrogenation set up actually used in this experiment 		 pages 211-216
6
 Exp. # 20: Reactivities of Some Alkyl Halides  pages 168-171
7
 Exp. # 23A: n-Butyl Bromide  pages 189-193
8
 Exp. # 58A:  Isolation of Essential Oils pages 523-530
9
 Exp. # 24:  4-Methylcyclohexene pages  193-197
10

Exp. # 56 Preparation of a C-4 or C-5 Acetate Ester (make-up lab)

  1. Equipment checkout
  2. Everyone attends checkout

male up lab: pages  124-132